Suite of Materials and Thin Film Analysis

Technique

Description

Typical Application

Signal Detected

Resolution

Imaging

Minimum Spot Size

Rutherford backscattering spectrometry (RBS)

Elemental  surface analysis and depth profiling

Thin film stoichiometry and near surface analysis of composition or impurities

Backscattered ions

 1E14/cm2
Depending upon mass of  target and impurity

No

1 mm
(1 µm for
µ-beam)

Ion Channeling

Elemental  analysis and depth profiling for single crystals

Lattice location of defects and impurities in single crystal material

Backscattered ions

See RBS

No

1 mm

(1 µm for
µ-beam)

Particle induced X-ray emission (PIXE)

Elemental surface analysis

Elemental analysis , 2-D map of trace impurities in Archeological, Biological and other bulk and thin films samples

Characteristic X-rays of elements

ppm to 100 ppb

~125 eV

Yes
(2-D elemental map)

1 mm

(1 µm for
µ-PIXE)

Nuclear reaction analysis   (NRA)

Elemental surface analysis for light elements

Depth profiling of light impurities, i.e. 1H, 2H, Be, B 15N, 18O

 Nuclear reaction products, i.e. proton, alpha, gamma, etc.)

 1E12/cm2
1 ppm
Reaction dependent

No

1 mm
(1 µm for
µ-beam)

Elastic recoil detection analysis (ERDA)

 Elemental surface analysis for light elements

Depth profiling of light impurities, i.e. 1H and 2H

Forward scattered recoiled atoms

0.1-1 atm%

No

2 mm

Atomic force microscopy (AFM)

Surface topography ad atomic scale imaging

Surface roughness, nanoparticle feature size, step heights

Tip deflection  from surface atomic morphology

< 5 Å

Yes

 

µ-Raman Spectroscopy (µ-Raman)

Inelastic scattering of light for chemical analysis

Molecular composition, strain in thin film, chemical analysis

Bond vibration
frequency

3 cm-1

2-D mapping

1 µm

Fourier-transform infrared spectroscopy (FTIR)

Infrared absorption spectroscopy for chemical analysis

Chemical and molecular structure analysis and thin film impurities

IR absorption

Sample dependent

No

 

 

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